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arxiv: 2106.01776 · v1 · pith:LTRAHOVTnew · submitted 2021-06-03 · ❄️ cond-mat.mtrl-sci

TEM observations on palladium samples aged up to 8 years under tritium

M. Segard , E. Leroy , B. Evin , S. Thiebaut , A. Fabre , S. Challet , V. Paul-Boncour This is my paper
classification ❄️ cond-mat.mtrl-sci
keywords agedagingbubblesexperimentspalladiumsamplessizetime
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Transmission electron microscopy (TEM) experiments were carried out on aged under tritium palladium powder samples. The experiments were devoted to the study of the evolution of 3He bubbles (size, density) appearing during aging. The study, using a new sample preparation, was focused for the first time on long aging time, up to 8 years. The TEM results indicated the presence of nanometer size bubbles (2 - 3 nm in diameter) with densities close to 5x10^23 m-3.

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    A simple mechanical and microstructural model using dislocation blocking predicts and fits the massive helium-3 release from aged palladium tritides.